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8.409 Aktuelle Fachpublikationen in Inorganic Chemistry

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Synthesis and Characterization of an Iridium Triphyrin Complex

23.09.2016 | Songlin Xue; Daiki Kuzuhara; Naoki Aratani; Hiroko Yamada, Inorganic Chemistry, 2016

A sandwich complex of iridium(III) benzotriphyrin (2) has been synthesized from free-base benzotriphyrin (1) and [IrCl(cod)]2 (COD = 1,5-cyclooctadiene). The COD ring was transformed from 1,5-COD to an η1,η3-C8H12 unit as a π-allyl ligand associated with the valence change of iridium from IrI to ...

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Prototropic μ-H8,9 and μ-H9,10 Tautomers Derived from the [nido-5,6-C2B8H11]− Anion

23.09.2016 | Oleg L. Tok; Zdenka Růžičková; Aleš Růžička; Drahomír Hnyk; Bohumil Štíbr, Inorganic Chemistry, 2016

Reported is an unusual tautomeric behavior within the [nido-5,6-C2B8H11]− (1a–) cage that has no precedence in the whole area of carborane chemistry. Isolated were two skeletal tautomers, anions [6-Ph-nido-5,6-C2B8H10-μ8,9]− (2d–) and [5,6-Me2-nido-5,6-C2B8H9-μ9,10]− (3b–), which differ in the ...

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A Bifunctional Europium–Organic Framework with Chemical Fixation of CO2 and Luminescent Detection of Al3+

22.09.2016 | Hang Xu; Bin Zhai; Chun-Shuai Cao; Bin Zhao, Inorganic Chemistry, 2016

A novel three-dimensional lanthanide–organic framework {[Eu(BTB)(phen)]·4.5DMF·2H2O}n (1) has been synthesized. Structural characterization suggests that framework 1 possesses one-dimensional channels with potential pore volume, and the large channels in the framework can capture CO2. ...

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Unique Axial Imidazole Geometries of Fully Halogenated Iron(II) Porphyrin Complexes: Crystal Structures and Mössbauer Spectroscopic Studies

22.09.2016 | Bin Hu; Mingrui He; Zhen Yao; Charles E. Schulz; Jianfeng Li, Inorganic Chemistry, 2016

The synthesis and characterization of several electron-poor iron(II) porphyrin (FeTFPPBr8) complexes with axial imidazole ligands are reported. The single-crystal X-ray structures have been studied by a combination of crystal packing and Hirshfeld surface calculations, which explained the unusual ...

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Antimicrobial Properties of Tris(homoleptic) Ruthenium(II) 2-Pyridyl-1,2,3-triazole “Click” Complexes against Pathogenic Bacteria, Including Methicillin-Resistant Staphylococcus aureus (MRSA)

22.09.2016 | Sreedhar V. Kumar; Synøve Ø. Scottwell; Emily Waugh; C. John McAdam; Lyall R. Hanton; Heather J. L. Brooks; James D. ..., Inorganic Chemistry, 2016

A series of tris(homoleptic) ruthenium(II) complexes of 2-(1-R-1H-1,2,3-triazol-4-yl)pyridine “click” ligands (R-pytri) with various aliphatic (R = butyl, hexyl, octyl, dodecyl, and hexdecyl) and aromatic (R = phenyl and benzyl) substituents was synthesized in good yields (52%–66%). The ...

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The Parent Li(OH)FeSe Phase of Lithium Iron Hydroxide Selenide Superconductors

22.09.2016 | Daniel N. Woodruff; Francesca Schild; Craig V. Topping; Simon J. Cassidy; Jack N. Blandy; Stephen J. Blundell; Amber ..., Inorganic Chemistry, 2016

Inorganic Chemistry DOI: 10.1021/acs.inorgchem.6b01734

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Highly Efficient Thermally Activated Delayed Fluorescence in Dinuclear Ag(I) Complexes with a Bis-Bidentate Tetraphosphane Bridging Ligand

22.09.2016 | Jin Chen; Teng Teng; Liju Kang; Xu-Lin Chen; Xiao-Yuan Wu; Rongmin Yu; Can-Zhong Lu, Inorganic Chemistry, 2016

A series of highly emissive neutral dinuclear silver complexes [Ag(PPh3)(X)]2(tpbz) (tpbz = 1,2,4,5-tetrakis(diphenylphosphanyl)benzene; X = Cl (1), Br (2), I (3)) was synthesized and structurally characterized. In the complexes, the silver atoms with tetradedral geometry are bridged by the tpbz ...

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A Kinetico-Mechanistic Study on CuII Deactivators Employed in Atom Transfer Radical Polymerization

22.09.2016 | Timothy J. Zerk; Manuel Martinez; Paul V. Bernhardt, Inorganic Chemistry, 2016

Copper complexes of tertiary amine ligands have emerged as the catalysts of choice in the extensively employed atom transfer radical polymerization (ATRP) protocol. The halide ligand substitution reactions of five-coordinate copper(II) complexes of tris[2-(dimethylamino)ethyl]amine (Me6tren), one ...

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Nonlinear-Optical Response of Prussian Blue: Strong Three-Photon Absorption in the IR Region

22.09.2016 | Jan K. Zaręba; Janusz Szeremeta; Magdalena Waszkielewicz; Marcin Nyk; Marek Samoć, Inorganic Chemistry, 2016

The nonlinear-optical properties of Prussian Blue nanoparticles have been evaluated with the use of femtosecond Z-scan measurements in the 1350–1750 nm range. This well-known inorganic pigment having interesting magnetic and electrochemical properties was found to be an efficient near-IR ...

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What Controls the Sign and Magnitude of Magnetic Anisotropy in Tetrahedral Cobalt(II) Single-Ion Magnets?

21.09.2016 | Shefali Vaidya; Subrata Tewary; Saurabh Kumar Singh; Stuart K. Langley; Keith S. Murray; Yanhua Lan; Wolfgang Wernsd ..., Inorganic Chemistry, 2016

A family of mononuclear tetrahedral cobalt(II) thiourea complexes, [Co(L1)4](NO3)2 (1) and [Co(Lx)4](ClO4)2 where x = 2 (2), 3 (3), 4 (4) (where L1 = thiourea, L2 = 1,3-dibutylthiourea, L3 = 1,3-phenylethylthiourea, and L4 = 1,1,3,3-tetramethylthiourea), has been synthesized using a rationally ...

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