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7.517 Aktuelle Fachpublikationen in Inorganic Chemistry

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Nonsteroidal Anti-inflammatory—Organometallic Anticancer Compounds

29.01.2016 | Emilia Păunescu; Sarah McArthur; Mylène Soudani; Rosario Scopelliti; Paul J. Dyson, Inorganic Chemistry, 2016

Compounds that combine metal-based drugs with covalently linked targeted organic agents have been shown, in some instances, to exhibit superior anticancer properties compared to the individual counterparts. Within this framework, we prepared a series of organometallic ruthenium(II)- and ...

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Crystal and Magnetic Structures of the Oxide Sulfides CaCoSO and BaCoSO

29.01.2016 | Edward J. T. Salter; Jack N. Blandy; Simon J. Clarke, Inorganic Chemistry, 2016

CaCoSO, synthesized from CaO, Co, and S at 900 °C, is isostructural with CaZnSO and CaFeSO. The structure is non-centrosymmetric by virtue of the arrangement of the vertex-sharing CoS3O tetrahedra which are linked by their sulfide vertices to form layers. The crystal structure adopts space group ...

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Postassembly Transformation of a Catalytically Active Composite Material, Pt@ZIF-8, via Solvent-Assisted Linker Exchange

29.01.2016 | Casey J. Stephenson; Joseph T. Hupp; Omar K. Farha, Inorganic Chemistry, 2016

2-Methylimidazolate linkers of Pt@ZIF-8 are exchanged with imidazolate using solvent-assisted linker exchange (SALE) to expand the apertures of the parent material and create Pt@SALEM-2. Characterization of the material before and after SALE was performed. Both materials are active as catalysts ...

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Synthesis of Nanocrystalline TiOF2 Embedded in a Carbonaceous Matrix from TiF4 and d-Fructose

29.01.2016 | Claudio Evangelisti; Mohammad Hayatifar; Fabio Marchetti; Marcello Marelli; Guido Pampaloni; Fabio Piccinelli, Inorganic Chemistry, 2016

Nanostructured titanium oxide difluoride embedded in a matrix of amorphous carbon was synthesized by pyrolysis of d-fructose in the presence of titanium tetrafluoride (optimal Ti/fructose molar ratio = 5.5), both in the solid state at ca. 150 °C and in suspension of 1,2-dichloroethane at reflux ...

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Luminescence Properties of SrZrO3/Tb3+ Perovskite: Host-Dopant Energy-Transfer Dynamics and Local Structure of Tb3+

29.01.2016 | Santosh Kumar Gupta; Partha Sarathi Ghosh; Ashok Kumar Yadav; Nimai Pathak; Ashok Arya; Shambhu Nath Jha; Dibyendu B ..., Inorganic Chemistry, 2016

SrZrO3 perovskite (SZP) was synthesized using gel-combustion route and characterized systematically using X-ray diffraction and time-resolved photoluminescence techniques. A detailed analysis of the optical properties of Tb3+ ions in SrZrO3 was performed to correlate them with the local ...

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Probing Effective Hamiltonian Operators by Single-Crystal EPR: A Case Study Using Dinuclear Cr(III) Complexes

29.01.2016 | Thorbjørn J. Morsing; Høgni Weihe; Jesper Bendix, Inorganic Chemistry, 2016

The use of a simple two-center model to describe exchange-coupled systems of various complexities is common in the field of coordination chemistry and molecular magnetism. In this work we investigate the applicability of this model experimentally, employing multifrequency, single-crystal EPR on ...

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Effects of the η5-C5H4iPr Ligand on the Properties Exhibited by Its Tungsten Nitrosyl Complexes

29.01.2016 | Diana Fabulyak; Rhett A. Baillie; Brian O. Patrick; Peter Legzdins; Devon C. Rosenfeld, Inorganic Chemistry, 2016

Reaction of Na[η5-C5H4iPr] with W(CO)6 in refluxing THF for 4 days generates a solution of Na[(η5-C5H4iPr)W(CO)3] that when treated with N-methyl-N-nitroso-p-toluenesulfonamide at ambient temperatures affords (η5-C5H4iPr)W(NO)(CO)2 (1) that is isolable in good yield as an analytically pure orange ...

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Theoretical Modeling of the Ligand-Tuning Effect over the Transition Temperature in Four-Coordinated FeII Molecules

29.01.2016 | Jordi Cirera; Eliseo Ruiz, Inorganic Chemistry, 2016

Spin-crossover molecules are systems of great interest due to their behavior as molecular level switches, which makes them promising candidates for nanoscale memory devices, among other applications. In this paper, we report a computational study for the calculation of the transition temperature ...

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Ionothermal Synthesis of MnAPO-SOD Molecular Sieve without the Aid of Organic Structure-Directing Agents

28.01.2016 | Hao Liu; Zhijian Tian; Lei Wang; Yasong Wang; Dawei Li; Huaijun Ma; Renshun Xu, Inorganic Chemistry, 2016

An SOD-type metalloaluminophosphate molecular sieve (denoted as SOD-Mn) was ionothermally synthesized by introducing manganese(II) cations into the reaction mixture via MnO–acid or MnO2–reductant reactions. Composition and structure analyses results show that two kinds of manganese(II) cations ...

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High-Frequency 13C and 29Si NMR Chemical Shifts in Diamagnetic Low-Valence Compounds of TlI and PbII: Decisive Role of Relativistic Effects

28.01.2016 | Jan Vícha; Radek Marek; Michal Straka, Inorganic Chemistry, 2016

The 13C and 29Si NMR signals of ligand atoms directly bonded to TlI or PbII heavy-element centers are predicted to resonate at very high frequencies, up to 400 ppm for 13C and over 1000 ppm for 29Si, outside the typical experimental NMR chemical-shift ranges for a given type of nuclei. The large ...

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