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8.806 Aktuelle Fachpublikationen in Inorganic Chemistry

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Unique Approach to Copper(I) Silylene Chalcogenone Complexes

13.01.2017 | Nasrina Parvin; Shiv Pal; Shabana Khan; Shubhajit Das; Swapan K. Pati; Herbert W. Roesky, Inorganic Chemistry, 2017

Silylene-S-thione [PhC(NtBu)2Si(═S)N(SiMe3)2] (2) and silylene-Se-selone [PhC(NtBu)2Si(═Se)N(SiMe3)2] (3) compounds were prepared from the silylene [PhC(NtBu)2SiN(SiMe3)2] (1) with 1 equiv of 1/8 S8 and 1 equiv of Se powder, respectively, in high yields. Furthermore, compounds 2 and 3 reacted ...

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Formation Mechanisms in β-Ca3(PO4)2–ZnO Composites: Structural Repercussions of Composition and Heat Treatments

13.01.2017 | Ponnusamy Nandha Kumar; José Maria da Fonte Ferreira; Sanjeevi Kannan, Inorganic Chemistry, 2017

Composites with varied proportions of β-Ca3(PO4)2 and ZnO were obtained through an in situ aqueous precipitation method under slightly basic (pH ≈ 8) conditions. The formation of β-Ca3(PO4)2 phase starts at an early heat-treatment stage (∼800 °C) and incorporates Zn2+ ions at both Ca2+(4) and ...

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Urea Metal–Organic Frameworks for Nitro-Substituted Compounds Sensing

13.01.2017 | Alireza Azhdari Tehrani; Leili Esrafili; Sedigheh Abedi; Ali Morsali; Lucia Carlucci; Davide M. Proserpio; Jun Wang; ..., Inorganic Chemistry, 2017

Urea groups are known to form strong hydrogen bonds with molecules containing atom(s) that can act as hydrogen bond acceptor(s). Thus, urea is a particularly interesting building block for designing receptors for neutral or charged guests. In the quest for new sensors with enhanced performance ...

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Reactions of Lithiated Diphosphanes R2P–P(SiMe3)Li (R = tBu and iPr) with [MeNacnacTiCl2·THF] and [MeNacnacTiCl3]. Formation and Structure of TitaniumIII and TitaniumIV β-Diketiminato Complexes Bearing the Side-on Phosphanylphosphido and Phosphanylphosphinidene Functionalities

13.01.2017 | Ł. Ponikiewski; A. Ziółkowska; J. Pikies, Inorganic Chemistry, 2017

β-Diketiminate complexes of TiIII-containing phosphanylphosphido ligands [MeNacnacTi(Cl){η2-P(SiMe3)-PR2}] (MeNacnac– = [Ar]NC(Me)CHC(Me)N[Ar]; Ar = 2,6-iPr2C6H3) were prepared by reactions of [MeNacnacTiCl2·THF] with lithium derivatives of diphosphanes R2P–P(SiMe3)Li (R = tBu, iPr) in toluene ...

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First-Order Phase Transition in BaNi2Ge2 and the Influence of the Valence Electron Count on Distortion of the ThCr2Si2 Structure Type

13.01.2017 | Viktor Hlukhyy; Dmytro Trots; Thomas F. Fässler, Inorganic Chemistry, 2017

Structural instability has a strong influence on the understanding of superconductivity in iron-containing 122 phases. Similar to the 122 iron-based high-temperature superconductors, the intermetallic compound BaNi2Ge2 undergoes an orthorhombic-to-tetragonal structural phase transition. The ...

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Effect of Water Coordination on Luminescent Properties of Pyrazine-Bridged Dinuclear Cu(I) Complexes

12.01.2017 | Atsushi Kobayashi; Ryuya Arata; Tomohiro Ogawa; Masaki Yoshida; Masako Kato, Inorganic Chemistry, 2017

Two luminescent pyrazine-bridged dinuclear Cu(I) complexes, namely, [{Cu(PPh3)2(H2O)}(μ-MeOpyz){Cu(PPh3)2(CH3CN)}](BF4)2 and [{Cu(PPh3)2(H2O)}(μ-MeOpyz){Cu(PPh3)2(H2O)}](BF4)2 (H2O–Cu2–AN and H2O–Cu2–H2O; PPh3 = triphenylphosphine, MeOpyz = 2-methoxypyrazine), were successfully synthesized and ...

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Synthesis, Structures, and CO Release Capacity of a Family of Water-Soluble PhotoCORMs: Assessment of the Biocompatibility and Their Phototoxicity toward Human Breast Cancer Cells

12.01.2017 | Indranil Chakraborty; Samantha J. Carrington; Graham Roseman; Pradip K. Mascharak, Inorganic Chemistry, 2017

Two manganese(I) carbonyl complexes derived from 2-(pyridyl)benzothiazole (pbt) and 1,10-phenanthroline (phen) release carbon monoxide (CO) under low-power broad-band visible-light illumination. CO photorelease from [Mn(CO)3(pbt)(PTA)]CF3SO3 (1, where PTA = 1,3,5-triaza-7-phosphaadamantane) is ...

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Ligand Design for Isomer-Selective Oxorhenium(V) Complex Synthesis

12.01.2017 | Jinyong Liu; Xiaoge Su; Mengwei Han; Dimao Wu; Danielle L. Gray; John R. Shapley; Charles J. Werth; Timothy J. Strat ..., Inorganic Chemistry, 2017

Recently, N,N-trans Re(O)(LN–O)2X (LN–O = monoanionic N–O chelates; X = Cl or Br prior to being replaced by solvents or alkoxides) complexes have been found to be superior to the corresponding N,N-cis isomers in the catalytic reduction of perchlorate via oxygen atom transfer. However, reported ...

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Structural Dependence of the Ising-type Magnetic Anisotropy and of the Relaxation Time in Mononuclear Trigonal Bipyramidal Co(II) Single Molecule Magnets

12.01.2017 | Feng Shao; Benjamin Cahier; Eric Rivière; Régis Guillot; Nathalie Guihéry; Victoria E. Campbell; Talal Mallah, Inorganic Chemistry, 2017

This paper describes the correlation between Ising-type magnetic anisotropy and structure in trigonal bipyramidal Co(II) complexes. Three sulfur-containing trigonal bipyramidal Co(II) complexes were synthesized and characterized. It was shown that we can engineer the magnitude of the Ising ...

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Decoding Proton-Coupled Electron Transfer with Potential–pKa Diagrams

11.01.2017 | Brian D. McCarthy; Jillian L. Dempsey, Inorganic Chemistry, 2017

Aqueous potential–pH diagrams, commonly called Pourbaix diagrams, were originally developed to study metal corrosion in the 1930s and 1940s. Pourbaix diagrams have since been widely adopted for use across chemistry disciplines, particularly for the study of aqueous proton-coupled electron ...

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