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8.611 Aktuelle Fachpublikationen in Inorganic Chemistry

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Transition-Metal-Complex Cationic Dyes Photosensitive to Two Types of 2D Layered Silver Bromides with Visible-Light-Driven Photocatalytic Properties

23.11.2016 | Cheng-Yang Yue; Xiao-Wu Lei; Yong-Fang Han; Xin-Xiu Lu; Ya-Wei Tian; Jing Xu; Xiao-Fan Liu; Xin Xu, Inorganic Chemistry, 2016

With mixed transition-metal (TM) complex, alkali-metal cations, or halogen anions as structure-directing agents, two types of two-dimensional (2D) layered inorganic–organic hybrid silver bromides were prepared and structurally characterized as K[TM(2,2-bipy)3]2Ag6Br11 (TM = Ni (1), Co (2), Zn ...

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Significantly Dense Two-Dimensional Hydrogen-Bond Network in a Layered Zirconium Phosphate Leading to High Proton Conductivities in Both Water-Assisted Low-Temperature and Anhydrous Intermediate-Temperature Regions

23.11.2016 | Daxiang Gui; Tao Zheng; Jian Xie; Yawen Cai; Yaxing Wang; Lanhua Chen; Juan Diwu; Zhifang Chai; Shuao Wang, Inorganic Chemistry, 2016

Inorganic Chemistry DOI: 10.1021/acs.inorgchem.6b02308

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“Straining” to Separate the Rare Earths: How the Lanthanide Contraction Impacts Chelation by Diglycolamide Ligands

23.11.2016 | Ross J. Ellis; Derek M. Brigham; Laetitia Delmau; Alexander S. Ivanov; Neil J. Williams; Minh Nguyen Vo; Benjamin Re ..., Inorganic Chemistry, 2016

The subtle energetic differences underpinning adjacent lanthanide discrimination are explored with diglycolamide ligands. Our approach converges liquid–liquid extraction experiments with solution-phase X-ray absorption spectroscopy (XAS) and density functional theory (DFT) simulations, spanning ...

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Selective Carbon Dioxide Adsorption by Two Robust Microporous Coordination Polymers

23.11.2016 | Litao An; Hao Wang; Feng Xu; Xin-Long Wang; Fangming Wang; Jing Li, Inorganic Chemistry, 2016

In the present work we report the design, synthesis, crystal structure determination, and adsorption properties of two new cadmium-based porous coordination polymers, [Cd(pda)0.5(spiro-4-py)0.5(HCOO)]·2H2O·DMF (compound 1, pda = p-phenylenediacetate, spiro-4-py = ...

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Rare Neutral Diphosphine Complexes of Scandium(III) and Yttrium(III) Halides

23.11.2016 | Marina Carravetta; Maria Concistre; William Levason; Gillian Reid; Wenjian Zhang, Inorganic Chemistry, 2016

Reaction of Me2PCH2CH2PMe2 or o-C6H4(PMe2)2 (L–L) with a suspension of ScI3 or YI3 in MeCN solution under rigorously anhydrous and oxygen-free conditions produced the highly unusual complexes [ScI3(L–L)2], [YI3(Me2PCH2CH2PMe2)2], and [YI3{o-C6H4(PMe2)2}2MeCN]. X-ray crystal structures reveal that ...

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Manganese Tricarbonyl Complexes with Asymmetric 2-Iminopyridine Ligands: Toward Decoupling Steric and Electronic Factors in Electrocatalytic CO2 Reduction

23.11.2016 | Steven J. P. Spall; Theo Keane; Joanne Tory; Dean C. Cocker; Harry Adams; Hannah Fowler; Anthony J. H. M. Meijer; Fr ..., Inorganic Chemistry, 2016

Manganese tricarbonyl bromide complexes incorporating IP (2-(phenylimino)pyridine) derivatives, [MnBr(CO)3(IP)], are demonstrated as a new group of catalysts for CO2 reduction, which represent the first example of utilization of (phenylimino)pyridine ligands on manganese centers for this purpose. ...

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Instability of the Ionic Conductor Li6BaLa2B2O12 (B = Nb, Ta): Barium Exsolution from the Garnet Network Leading to CO2 Capture

23.11.2016 | Cyrille Galven; Gwenaël Corbel; Françoise Le Berre; Marie-Pierre Crosnier-Lopez, Inorganic Chemistry, 2016

The instability of the two garnets Li6BaLa2B2O12 (B = Nb, Ta) has been studied on samples prepared in powder form by solid-state reaction. For this study, we coupled different techniques: powder X-ray diffraction, IR spectrometry, thermal analysis, transmission electron microscopy, and complex ...

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Effect of Internal Pressure and Temperature on Phase Transitions in Perovskite Oxides: The Case of the Solid Oxide Fuel Cell Cathode Materials of the La2–xSrxCoTiO6 Series

23.11.2016 | Alejandro Gómez-Pérez; Markus Hoelzel; Álvaro Muñoz-Noval; Flaviano García-Alvarado; Ulises Amador, Inorganic Chemistry, 2016

The symmetry of the room-temperature (RT) structure of title compounds La2–xSrxCoTiO6−δ changes with x, from P21/n (0 ≤ x ≤ 0.2) to Pnma (0.3 ≤ x ≤ 0.5) and to R3̅c (0.6 ≤ x ≤ 1). For x = 1 the three pseudocubic cell parameters become very close suggesting a transition to a cubic structure for ...

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Computational Gas-Phase Formation Enthalpy and Electron Affinity for Platinum Hexafluoride: Is Gaseous PtF6 Diamagnetic because of a Relativistic Effect?

23.11.2016 | Robson Fernandes De Farias, Inorganic Chemistry, 2016

In the present work, a computational thermochemistry study (semiempirical, PM6 method) for platinum hexafluoride (PtF6) is performed. The gas-phase formation enthalpy (ΔfH°) and electron affinity are calculated and the results compared with the experimental data. A calculated ΔfH°(g) value of ...

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Transformation of One-Dimensional Achiral Structure to Three-Dimensional Chiral Structure: Mechanistic Study and Catalytic Activities of Chiral Structure

23.11.2016 | Purna Chandra Rao; Sonu Pratap Chaudhary; Denis Kuznetsov; Sukhendu Mandal, Inorganic Chemistry, 2016

We have isolated two copper-based coordination polymers through solvent diffusion and solvothermal methods using copper salt, furan dicarboxylic acid (FDC), 4,4′-bipyridine (bpy) in MeOH/ethylene glycol, and water solvents. Compound 1 is adopting P21/c space group and adopts a one-dimensional ...

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