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48.746 Aktuelle Fachpublikationen zum Thema temperature

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Radiation-induced radicals in different polymorphic modifications of d-mannitol: Structure, conformations and dosimetric implications

12.10.2015 | Author(s): Ilya S. Sosulin, Ekaterina S. Shiryaeva, Vladimir I. Feldman, Radiation Physics and Chemistry, 2015

Publication date: December 2015 Source:Radiation Physics and Chemistry, Volume 117 Author(s): Ilya S. Sosulin, Ekaterina S. Shiryaeva, Vladimir I. Feldman The structure and conformation of radicals produced by X-ray irradiation of three polymorphic forms of d-mannitol were ...


Phase equilibria in the Tb-Mg-Co system at 500°C, crystal structure and hydrogenation properties of selected compounds

11.10.2015 | Author(s): V.V. Shtender, R.V. Denys, I.Yu. Zavaliy, O.Ya. Zelinska, V. Paul-Boncour, V.V. Pavlyuk, Journal of Solid State Chemistry, 2015

Publication date: December 2015 Source:Journal of Solid State Chemistry, Volume 232 Author(s): V.V. Shtender, R.V. Denys, I.Yu. Zavaliy, O.Ya. Zelinska, V. Paul-Boncour, V.V. Pavlyuk The isothermal section of the Tb–Mg–Co phase diagram at 500°C has been built on the basis of XRD ...


Isolation of organomercury(II) azides stabilized by intramolecular coordination

11.10.2015 | Author(s): Shikha Das, Harkesh B. Singh, Ray J. Butcher, Journal of Organometallic Chemistry, 2015

Publication date: 15 December 2015 Source:Journal of Organometallic Chemistry, Volumes 799–800 Author(s): Shikha Das, Harkesh B. Singh, Ray J. Butcher A series of arylmercury azides stabilized by o-imino/amino coordinating groups has been synthesized. Synthesis of the room temperature ...


In Situ Studies of Surface‐Plasmon‐Resonance‐Coupling Sensor Mediated by Stimuli‐Sensitive Polymer Linker

09.10.2015 | Ji‐Eun Lee, Kyungwha Chung, Jumi Lee, Kwanwoo Shin, Dong Ha Kim, Advanced Functional Materials, 2015

Hybrid plasmonic nanostructures comprising gold nanoparticle (AuNP) arrays separated from Au substrate through a temperature‐sensitive poly(N‐isopropylacrylamide) (PNIPAM) linker layer are constructed, and unique plasmonic‐coupling‐based surface plasmon resonance (SPR) sensing properties are ...


Mechanical Alloying and Spark Plasma Sintering of BiCuSeO Oxyselenide: Synthesis Process and Thermoelectric Properties

09.10.2015 | Jin Wu, Fu Li, Tian‐Ran Wei, Zhenhua Ge, Feiyu Kang, Jiaqing He, Jing‐Feng Li, Journal of the American Ceramic Society, 2015

BiCuSeO is a promising thermoelectric material but needs a complicated synthesis process. In this work, fine‐grained BiCuSeO samples with high phase purity were synthesized by a combination of mechanical alloying (MA) and spark plasma sintering (SPS). It is found that BiCuSeO compounds can be ...


Syntheses of Isoquinoline and Substituted Quinolines in Charged Microdroplets

09.10.2015 | Shibdas Banerjee, Richard N. Zare, Angewandte Chemie International Edition, 2015

Abstract A Pomeranz–Fritsch synthesis of isoquinoline and Friedländer and Combes syntheses of substituted quinolines were conducted in charged microdroplets produced by an electrospray process at ambient temperature and atmospheric pressure. In the bulk phase, all of these reactions are known ...


Retardation of shape change of Au nanorods using photo‐cross‐linkable ligands

09.10.2015 | Scott P. O. Danielsen, Jihoon Choi, Russell J. Composto, Journal of Polymer Science Part B: Polymer Physics, 2015

ABSTRACT The thermal reshaping of gold nanorods has been slowed by grafting a diblock copolymer [P(S‐b‐S‐N3)] containing an outer polystyrene (PS) brush and a short, inner photo‐cross‐linkable PS‐azide block. The P(S‐b‐S‐N3)‐Au NRs were dispersed in a PS thin film and reshaping was ...


Luminescent Thermochromism in a Gold(I)–Copper(I) Phosphine–Pyridine Complex

08.10.2015 | Kelly Chen, Vincent J. Catalano, European Journal of Inorganic Chemistry, 2015

Abstract The AuI complex [Au(Ph2PCH2py)2]BF4 (1) was prepared by mixing (tetrahydrothiophene)gold(I) chloride with 2‐[(diphenylphosphino)methyl]pyridine (Ph2PCH2py) in dichloromethane. The addition of [Cu(NCCH3)4]BF4 to 1 produced green‐luminescent [AuCu(Ph2PCH2py)2(NCCH3)2](BF4)2 (2). When ...


Solvent‐Free Ball‐Milling Biginelli Reaction by Subcomponent Synthesis

08.10.2015 | Prasit Kumar Sahoo, Anima Bose, Prasenjit Mal, European Journal of Organic Chemistry, 2015

Abstract We report here an understanding of systems chemistry on small molecules through covalent mechanochemistry. As a proof‐of‐concept, the multicomponent Biginelli reaction by subcomponent synthesis was considered as a model system. Reactions were performed under solvent‐free, metal‐free, ...


Corrosion product transformations in alkaline baths under pressure and high temperature: The sub‐critical stabilisation of marine iron artefacts stored under atmospheric conditions

08.10.2015 | M. Bayle, P. de Viviés, J.‐B. Memet, E. Foy, P. Dillmann, D. Neff, Materials and Corrosion, 2015

In the context of conservation of ferrous cultural heritage, dechlorination processes of archaeological iron artefacts are studied in subcritical conditions which consist of immerging an artefact inside an alkaline bath under pressure (30 bar) and temperature (160 °C). Submarine archaeological ...


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