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5.397 Aktuelle Fachpublikationen zum Thema temperature

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Tautomerism of a compartmental Schiff base ligand and characterization of a new heterometallic CuII–DyIII complex — Synthesis, structure and magnetic properties

05.01.2015 | Author(s): B. Cristóvão , B. Miroslaw, Inorganic Chemistry Communications, 2015

Publication date: February 2015 Source:Inorganic Chemistry Communications, Volume 52 Author(s): B. Cristóvão , B. Miroslaw A crystal structure of a compartmental ligand N,N′-bis(2,3-dihydroxybenzylidene)-1,3-diaminopropane (H4L=C17H18N2O4) (1) containing N2O2-inner and O4-outer ...


Effective synthesis of novel O-acetylated compounds over ZrO2-Al2O3 solid acid

04.01.2015 | Author(s): N. Thimmaraju , S.Z. Mohamed Shamshuddin , S.R. Pratap , K. Shyam Prasad, Arabian Journal of Chemistry, 2015

Publication date: Available online 3 January 2015 Source:Arabian Journal of Chemistry Author(s): N. Thimmaraju , S.Z. Mohamed Shamshuddin , S.R. Pratap , K. Shyam Prasad The solid acids such as Al2O3, ZrO2 and ZrO2-Al2O3 containing different ZrO2 loadings (10-100 mol%) were prepared by ...


Ionic liquid [tbmim]Cl2/AlCl3 under ultrasonic irradiation towards synthesis of 1,4-DHP’s

04.01.2015 | Author(s): B. Palakshi Reddy , K. Rajesh , V. Vijayakumar, Arabian Journal of Chemistry, 2015

Publication date: January 2015 Source:Arabian Journal of Chemistry, Volume 8, Issue 1 Author(s): B. Palakshi Reddy , K. Rajesh , V. Vijayakumar One pot, three-component synthesis of 1,4-dihydropyridines using ionic liquid 3,3′-thionyl-bis-1,1′-methylimidazolium chloroaluminate ...


Cardo fluorene based semifluorinated co-poly(arylene ether)s: Synthesis, characterization and dielectric properties

04.01.2015 | Author(s): Sayantani Saha , Ershad Ali Mistri , Debaditya Bera , Susanta Banerjee, Materials Chemistry and Physics, 2015

Publication date: 15 February 2015 Source:Materials Chemistry and Physics, Volume 152 Author(s): Sayantani Saha , Ershad Ali Mistri , Debaditya Bera , Susanta Banerjee Three new co-poly(arylene ether)s (PAE) containing cardo fluorene moiety in the main chain and pendent trifluoromethyl ...


Influence of selenization temperature on synthesis, morphology, and properties of nanostructured CoSe2 films

03.01.2015 | Jen‐Bin Shi, Po‐Feng Wu, Chia‐Tze Kao, Ming‐Way Lee, Chih‐Chieh Chan, Ping‐Chang Yang, Cheng‐Li Lin, Rui‐Yo Huang, Y ..., Crystal Research and Technology, 2015

Nanostructured cobalt selenide (CoSe2) thin films were deposited on a glass substrate using the selenization of Co films at different selenization temperatures (300 °C, 400 °C, and 500 °C) in a pure Se vapor for two hours. The morphology and structure of the as‐deposited films shows that the ...


Temperature-Mediated Polymorphism in Molecular Crystals: The Impact on Crystal Packing and Charge Transport

02.01.2015 | Loah A. Stevens; Katelyn P. Goetz; Alexandr Fonari; Ying Shu; Rachel M. Williamson; Jean-Luc Brédas; Veaceslav Corop ..., Chemistry of Materials, 2015

We report a novel synthesis to ultra high purity 7,14-bis((trimethylsilyl)ethynyl)dibenzo[b,def]-chrysene (TMS-DBC) and the use of this material in the growth of single crystals by solution and vapor deposition techniques. We observe that the substrate temperature has a dramatic impact on the ...


Materials, Vol. 8, Pages 149-161: Synthesis of Co3O4 Cotton-Like Nanostructures for Cholesterol Biosensor

31.12.2014 | Elhag, Sami ; Ibupoto, Zafar Hussain; Nour, Omer ; Willander, Magnus, Materials, 2014

The use of templates to assist and possess a control over the synthesis of nanomaterials has been an attractive option to achieve this goal. Here we have used sodium dodecyl sulfate (SDS) to act as a template for the low temperature synthesis of cobalt oxide (Co3O4) nanostructures. The use of SDS ...


Aerosol-Assisted Controlled Packing of Silica Nanocolloids: Templateless Synthesis of Mesoporous Silicates with Structural Tunability and Complexity

31.12.2014 | Kyungmin Min; Chang Hyuck Choi; Myoung Yeob Kim; Minkee Choi, Langmuir, 2014

A template-free synthesis method for mesoporous and macro-/mesoporous hierarchically porous silicates with remarkable structural tunability and complexity is presented. SiO2 nanocolloids having diameters of 3.0–29 nm were prepared as a primary building block by using extended Stöber synthesis, ...


Synthesis of sulfonamides via I2-mediated reaction of sodium sulfinates with amines in aqueous medium at room temperature

30.12.2014 | Gao-Qing Yuan; Xiaojun Pan; Jian Gao; Juan Liu; Junyi Lai; Huanfeng Jiang, Green Chemistry, 2014

An efficient I2-mediated approach to the synthesis of sulfonamides at room temperature using water as the solvent has been developed. This method for the synthesis of sulfonamides is quite convenient and environment friendly. In addition, the purification procedure of the desired products becomes ...


TBPB-promoted metal-free synthesis of thiophosphinate/phosphonothioate by direct P–S bond coupling

30.12.2014 | Jichao Wang; Xin Huang; Zhangqin Ni; Sichang Wang; Jun Wu; Yuanjiang Pan, Green Chemistry, 2014

An efficient method for the direct coupling of thiol/thiophenol with H-phosphine oxides or H-phosphinate esters is reported. Without using any metallic catalyst, the direct sulfur–phosphorus bond coupling reaction was promoted using tert-butyl peroxybenzoate in the presence of KI at room ...


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