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Two Nickel(II) Coordination Polymers Based on Tri(p‐carboxyphenyl) phosphane Oxide with Highly Selectively and Sensitively Detection of Acetone

15.01.2018 | Kegong Fang, liangqin Huo, Lingling Gao, Fuqiang An, Jianfeng Gao, Liming Fan, tuoping hu, Zeitschrift für anorganische und allgemeine Chemie, 2018

Abstract. Two nickel (II) coordination polymers, namely, {[Ni1/2(TPO)1/3(bib)1/2(H2O)]*H2O}n (1), and [Ni(HTPO)(bpy)(H2O)2]n (2), have been assembled from tripodal ligand of tripodal tri(p‐carboxyphenyl) phosphane oxide (H3TPO) and two N‐donors (bib = 1,4‐bis(imidazolyl)benzene, and bpy = ...


Polymeric Copper(II) Paddlewheel Carboxylate: Structural Description, Electrochemistry, and DNA‐binding Studies

15.01.2018 | Muhammad Iqbal, Sqib Ali, Muhammad Nawaz Tahir, Zeitschrift für anorganische und allgemeine Chemie, 2018

A polymeric complex of copper(II) was isolated and purified from the self‐assembly of CuSO4 and 2‐phenyl acetate in aqueous medium. It was characterized through FT‐IR, UV/Vis, electron spin resonance, electrochemical solution studies, and powder and single crystal XRD techniques. The structure ...


Detection and Quantifiable Evaluation of Copper(II) ions through Luminescent Sensing between Two Homologous Metal‐organic Frameworks

15.01.2018 | Jiang Li, Chang-Peng Men, Yu-Qing Luo, Shao-Jie Mo, Wen-Huan Huang, Lin Cui, Zeitschrift für anorganische und allgemeine Chemie, 2018

Two luminescent metal‐organic frameworks (LMOFs), namely, [Cd2(DDCPB)·(DMF)2·H2O]n (CHD‐1) and [Zn2(DDCPB)·(DMA)2]n·n(DMA) (CHD‐2), have been solvothermally constructed, which present structural diversity. Single crystal X‐ray diffraction analysis indicates that they consist of ...


Solar light photocatalytic degradation of Malachite Green by hydrothermally synthesized Strontium Arsenate Nanomaterial through response surface methodology

11.01.2018 | shahin khademinia, Leila kafi-ahmadi, Zeitschrift für anorganische und allgemeine Chemie, 2018

Nanostructured Sr2As2O7 samples were synthesized by hydrothermal crystal growth reactions between Sr(NO3)2 and As2O3 with different stoichiometric Sr:As molar ratios as 1:1 (S1), 1:2 (S2) and 2:1 (S3). The synthesized nanomaterials were characterized by powder X‐ray diffraction (PXRD) technique ...


The Specific Impulse as an Important Parameter for Predicting Chemical High Explosives Performance

10.01.2018 | Dany FREM, Zeitschrift für anorganische und allgemeine Chemie, 2018

The plate dent test is one of the most useful tools used by experimenters for the determination of explosive performance. However, performing the test for every new composition is certainly tedious and time consuming. Hence, the aim of the present study was to introduce a model from which the ...


Crystal Structure and Characterization of Two Layered Copper(II) Coordination Polymers with Anions of 3‐Phosphonopropionic Acid and (RS)‐2‐Phosphonobutyric Acid

09.01.2018 | Christian Robl, Roberto Köferstein, Michael Arnold, Zeitschrift für anorganische und allgemeine Chemie, 2018

Abstract: Blue single crystals of Cu[µ3‐O3P(CH2)2COOH]2H2O (1) and Cu[(RS)‐µ3‐O3PCH(C2H5)COOH]3H2O (2) have been prepared in aqueous solutions (pH = 2.5‐3.5). 1: Space group Pbca (no. 61) with a = 812.5(2), b = 919.00(9), c = 2102.3(2) pm. Cu2+ is five‐fold coordinated by three oxygen atoms ...


Gadolinium (III) 2‐benzoyl‐1,1,3,3‐tetracyanopropenide diacetate: synthesis and crystal structure

28.12.2017 | Sergey Karpov, Yakov Sergeevich Kauykov, Arthur Alexandrovich Grigor'ev, Victor Alexandrovich Tafeenko, Zeitschrift für anorganische und allgemeine Chemie, 2017

2‐Acyl‐1,1,3,3‐tetracyanopropenides (ATCN) is a stable organic salts, containing the carbonyl group in addition to the tetracyanoallyl (TCA) fragment in the anion. TCA anions are known as bridging ligands with variable denticity with potential application in organic electronics and as a ionic ...


Facile Syntheses of pure Uranium(III) Halides: UF3, UCl3, UBr3, and UI3

20.12.2017 | Stefan S Rudel, H. Lars Deubner, Benjamin Scheibe, Matthias Conrad, Florian Kraus, Zeitschrift für anorganische und allgemeine Chemie, 2017

Herein we describe a convenient lab scale synthesis for pure and solvent‐free binary uranium(III) halides UCl3, UBr3 and UI3. This is achieved by the reduction of the respective uranium(IV) halides with elemental silicon in borosilicate ampoules at moderate temperature. The silicon tetrahalides ...


Self‐Assembly of Discrete Copper(I)‐Halide Complexes with Diacylthioureas

18.12.2017 | Herbert W. Roesky, Xianhui Hou, Fanfan Wang, Li Han, Xia Pan, Haipu Li, Ying Yang, Zeitschrift für anorganische und allgemeine Chemie, 2017

Three diacylthioureas 1,4‐C6H4[C(O)NHC(S)NHAr]2 (Ar = 2,6‐iPr2C6H3) (L1, 1), 1,3‐C6H4[C(O)NHC(S)NHAr]2 (L2, 2) and 1,3‐C6H4[C(O)NHC(S)NHArꞌ]2 (Arꞌ = 2,6‐Me2C6H3) (L3, 3) were synthesized and characterized. The CuI complexes from the reactions of bipodal ligands Ln with CuX (X = Cl, Br, I) were ...


In celebration of Thomas Schleid's 60th birthday

05.12.2017 | Zeitschrift für anorganische und allgemeine Chemie, 2017


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